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Solid-phase microextraction versus single-drop microextraction for the analysis of nitroaromatic explosives in water samples

Psyllaki Eleftheria, Kalogerakis Nikos

Πλήρης Εγγραφή


URI: http://purl.tuc.gr/dl/dias/E736589D-ED2A-4E16-B559-F294DA2C8E86
Έτος 2001
Τύπος Δημοσίευση σε Περιοδικό με Κριτές
Άδεια Χρήσης
Λεπτομέρειες
Βιβλιογραφική Αναφορά E. Psillakis and N.Kalogerakis,"Solid-phase microextraction versus single-drop microextraction for the analysis of nitroaromatic explosives in water samples," J. Chrom. A, vol. 938, no.1-2, pp. 113–120, Dec. 2001. doi:10.1016/S0021-9673(01)01417-0 https://doi.org/10.1016/S0021-9673(01)01417-0
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Περίληψη

This paper compares solid-phase microextraction (SPME) with a recently developed extraction method called single-dropmicroextraction (SDME) for the analysis of nitroaromatic explosives in water samples. The two techniques are examined interms of procedure, chromatographic analysis and method performance. All practical considerations for both techniques arealso reviewed. SPME requires dedicated apparatus and is relatively expensive, as the fiber’s lifetime is limited. However, ithas the advantages over SDME that it can be easily used for headspace analysis and has lower detection limits for all thetarget analytes. SDME requires more elaborate manual operations, thus affecting linearity and precision.

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