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Technical University of Crete
Technical University of Crete
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| URI | http://purl.tuc.gr/dl/dias/D349CD5D-7DEC-4B16-AAC4-129DE34610B5 | - |
| Identifier | https://doi.org/10.1016/S0165-9936(03)01007-0 | - |
| Language | en | - |
| Title | Developments in liquid-phase microextraction | en |
| Creator | E Psillakis | en |
| Creator | N Kalogerakis | en |
| Publisher | Elsevier | en |
| Content Summary | The development of faster, simpler, inexpensive and more environmentally friendly sample-preparation techniques is an important issue in chemical analysis. Recent research trends involve miniaturisation of the traditional liquid-liquid extraction (LLE) principle by greatly reducing the acceptor-to-donor phase ratio. One of the emerging techniques in this area is liquid-phase microextraction (LPME), where a hollow fibre impregnated with an organic solvent is used to accommodate or protect microvolumes of acceptor solution. This novel methodology proved to be an extremely simple, low-cost and virtually solvent-free sample-preparation technique, which provided a high degree of selectivity and enrichment by additionally eliminating the possibility of carry-over between runs. This article presents the different modes and hollow-fibre configurations of LPME, followed by an up-to-date summary of its applications. The most important parameters and practical considerations for method optimisation are also discussed. The article concludes with a comparison of this novel method with solid-phase microextraction (SPME) and single-drop microextraction (SDME). | en |
| Type of Item | Peer-Reviewed Journal Publication | en |
| Type of Item | Δημοσίευση σε Περιοδικό με Κριτές | el |
| License | http://creativecommons.org/licenses/by/4.0/ | en |
| Date of Item | 2015-09-23 | - |
| Date of Publication | 2003 | - |
| Bibliographic Citation | E. Psillakis, N. Kalogerakis , " Developments in liquid-phase microextraction ", Tr. in An. Chem.,vol. 22, no.9, pp. 565–574,2003.doi :10.1016/S0165-9936(03)01007-0 | en |
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