Institutional Repository
Technical University of Crete
Technical University of Crete
EN
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EL
| URI | http://purl.tuc.gr/dl/dias/4F402DAC-2679-4721-93E5-1A2832BEAB8B | - |
| Identifier | https://doi.org/10.1016/S0021-9673(00)01017-7 | - |
| Identifier | http://www.sciencedirect.com/science/article/pii/S0021967300010177 | - |
| Language | en | - |
| Extent | 9 pages | en |
| Title | Application of solvent microextraction to the analysis of nitroaromatic explosives in water samples | en |
| Creator | Psyllaki Eleftheria | en |
| Creator | Ψυλλακη Ελευθερια | el |
| Creator | Kalogerakis Nikos | en |
| Creator | Καλογερακης Νικος | el |
| Publisher | Elsevier | en |
| Content Summary | The application of solvent microextraction to the analysis of nitroaromatic explosives is presented. Extraction of 11 nitroaromatics was achieved by suspending 1 ml of organic solvent to the tip of a microsyringe in a stirred aqueous solution. Parameters such as extraction solvent, stirring rate, salt concentration and sampling time were studied and optimized. The limits of detection using bench-top quadrupole mass spectrometry and short extraction times (15 min) were found to be between 0.08 and 1.3 mg/ l and the relative standard deviations ranged between 4.3 and 9.8%. Although precision and accuracy of quantification of the method are still needed, solvent microextraction proved to be a fast, simple and inexpensive tool for preconcentration and matrix isolation of nitroaromatics on a microscale | en |
| Type of Item | Peer-Reviewed Journal Publication | en |
| Type of Item | Δημοσίευση σε Περιοδικό με Κριτές | el |
| License | http://creativecommons.org/licenses/by/4.0/ | en |
| Date of Item | 2015-09-24 | - |
| Date of Publication | 2001 | - |
| Subject | Explosives | en |
| Subject | Nitroaromatic compounds | en |
| Bibliographic Citation | E. Psillakis and N. Kalogerakis, "Application of solvent microextraction to the analysis of nitroaromatic explosives in water samples, " J. Chromatogr. A, vol. 907, no. 1-2, pp. 211–219, Jan. 2001. doi: 10.1016/S0021-9673(00)01017-7 | en |
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