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Technical University of Crete
Technical University of Crete
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| URI | http://purl.tuc.gr/dl/dias/BB3D22BA-88EE-4E5E-A9BD-DA670657C1CE | - |
| Identifier | https://doi.org/10.1016/j.culher.2020.06.005 | - |
| Identifier | https://www.sciencedirect.com/science/article/pii/S1296207420303939 | - |
| Language | en | - |
| Extent | 10 pages | en |
| Extent | 3,33 megabytes | en |
| Title | Morphological characterization of water-based nanolime dispersions | en |
| Creator | Michalopoulou Anastasia | en |
| Creator | Μιχαλοπουλου Αναστασια | el |
| Creator | Maravelaki Pagona | en |
| Creator | Μαραβελακη Παγωνα | el |
| Creator | Kilikoglou, Vassilis | en |
| Creator | Karatasios, Ioannis | en |
| Publisher | Elsevier | en |
| Description | This research is co-financed by Greece and the European Union (European Social Fund- ESF) through the Operational Programme «Human Resources Development, Education and Lifelong Learning» in the context of the project “Strengthening Human Resources Research Potential via Doctorate Research” (MIS-5000432), implemented by the State Scholarships Foundation (IKY). | en |
| Description | Η έρευνα συγχρηματοδοτείται από την Ελλάδα και την Ευρωπαϊκή Ένωση (Ευρωπαϊκό Κοινωνικό Ταμείο - ΕΚΤ) στα πλαίσια του Επιχειρησιακού Προγράμματος «Ανάπτυξη Ανθρώπινου Δυναμικού, Εκπαίδευση και Δια βίου Μάθηση» Πράξη «Ενίσχυση του ανθρώπινου ερευνητικού δυναμικού μέσω της υλοποίησης διδακτορικής έρευνας» (MIS 5000432), που υλοποιήθηκε από το Ίδρυμα Κρατικών Υποτροφιών (IKY). | el |
| Content Summary | This paper studies the morphological characteristics of calcium hydroxide nanoparticles in water based dispersions, produced following the main bottom-up (CaCl2/NaOH replacement reaction) and top-down methodologies. The work focuses on the effect of three different surfactants (TritonX-100, n-octylamine and amylamine) on the morphological characteristics of the resulting Ca(OH)2 nanoparticles and compares them with the ones produced in a mixture of water and 2-propanol. Moreover, in an attempt to approach the compatibility enhancement with siliceous stones, a calcium hydroxide—TEOS composite was also studied. The morphological, chemical and the mineralogical characterization of the nanoparticles produced were carried out by electron microscopy (SEM), dynamic light scattering (DLS), Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD). It is shown that the modifications induced by the production methodologies limited the agglomeration phenomena and altered the morphological characteristics of nanoparticles, when compared to the results obtained by the original bottom-up method, resulting in the synthesis of hexagonal, plate-like, rounded and angular portlandite nanoparticles. The size range of the nanoparticles extended from 60 to 350 nm. | en |
| Type of Item | Peer-Reviewed Journal Publication | en |
| Type of Item | Δημοσίευση σε Περιοδικό με Κριτές | el |
| License | http://creativecommons.org/licenses/by/4.0/ | en |
| Date of Item | 2021-04-07 | - |
| Date of Publication | 2020 | - |
| Subject | Nanolime | en |
| Subject | Conservation | en |
| Subject | Consolidation | en |
| Subject | Surfactants | en |
| Subject | Electron microscopy | en |
| Bibliographic Citation | A. Michalopoulou, P.-N. Maravelaki, V. Kilikoglou and I. Karatasios, “Morphological characterization of water-based nanolime dispersions,” J. Cult. Herit., vol. 46, pp. 11–20, Nov.-Dec. 2020., doi: 10.1016/j.culher.2020.06.005 | en |
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